Development of Beta Titanium Alloys by Spark Plasma Sintering

M.A. Lagos, A. Amigo, A. Vicente, Iñigo Agote

Research output: Contribution to conferencePaperpeer-review

Abstract

Beta titanium alloys have attracted considerable attention especially for orthopedic implants applications owing to their unique combination of low elastic modulus, superior bio-corrosion resistance and excellent biocompatibility. However, the PM production of these alloys is difficult due to the significant amount of refractory metals (Ta, Mo, Zr, Nb, etc). This work presents a processing route combining mechanical mixing of elemental powders (pre-alloying) and Spark Plasma Sintering in order to obtain fully dense materials with homogeneous microstructure. Two different compositions (TiMo and TiNb) with high amount of alloying elements were developed. The alloys were sintered at temperatures between 1100 and 1250ºC. The phases were evaluated by X-ray diffraction and diffraction of backscattered electrons, appreciating its mechanical properties by micro-hardness and bending tests. A transformation to Beta Titanium is obtained predominantly with a small grain size, and micro-hardness in the order of forged materials.
Original languageEnglish
Publication statusPublished - 2017
EventInternational Powder Metallurgy Congress and Exhibition, Euro PM 2017 - Milan, Italy
Duration: 1 Oct 20174 Oct 2017

Conference

ConferenceInternational Powder Metallurgy Congress and Exhibition, Euro PM 2017
Country/TerritoryItaly
CityMilan
Period1/10/174/10/17

Keywords

  • Mechanical mixing
  • TNZT
  • Ti-Mo alloys
  • EBSD
  • Microstructure

Project and Funding Information

  • Funding Info
  • the Spanish Ministry of Economy and Competitiveness through the financial support of the research project MAT2014-53764-C3-1-R and the Generalitat Valenciana through support PROMETEO/2016/040. The European Commission via FEDER funds that have allowed the purchase of equipment for research and Microscopy Service at the Polytechnic University of Valencia.

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